a) Composition in sample b) Concentration of elements in sample c) Relative mass of atoms d) Properties of sample. �� Mass spectrometers are used to determine which of the following? **The mass to charge ratio ( m/z) is used to describe ions observed in mass spectrometry.By convention, m is the numerical value for the mass of the ion and z is the numerical value for the charge of the ion. Explain how ionisation is achieved. Then Zr-91, and the least abundant is Zr-96 1. THE MASS SPECTROMETER 1. What does each peak represent? %PDF-1.6 %���� %%EOF 4. /mmz�>�I_�E�J���ֹ||5_�ô�N��В�����9�O�X��gb4n��85�� 0 )�!��S�']Vn�wR�M.�:F�p����{`v�.V@Aw�r,����T��B�b�WO�'�Wu=l��^Q��~'�VA�+�� Tm�9:?F��|�����އGn,�n�8u$�z�{�~������J�m׆��k�{�(QY�C'��䖴��%j^K��o ���w�\0�1�p@�.b�'��� The diagram, taken from the Chemguide page, shows the main parts of a mass spectrometer. 3418 0 obj <> endobj Mass Spectrometer Questions & Answers. Ou�q8�ң�TH(/r�wP=[+���S���`�/qQ��� ��Ш2Q���6K������. endstream endobj startxref 2. a) m/z is the mass/charge ratio - the mass of the ion divided by its charge. 3 Mass Relationships in Chemical Reactions MASS SPECTROMETRY Use the spectrum below to answer questions 1-5. b) Zirconium has 5 isotopes with relative isotopic masses of 90, 91, 92, 94 and 96. 3���IV$��/� Since the x-axis is labeled mass number (amu), what can we assume about the charge? How is this ionisation done? Answer: c. Explanation: Mass spectrometers are used to determine the relative mass of atoms and molecules. 2. 204 196 198 199 200 202 202 mass number (anti-a) 1. Name the h�bbd```b``���7@$�^�"YZ@${$�\�H2�� �� ���f`bd�}���H�?×� �� 4 [4 marks] 01.2 A second method of ionising samples in time of flight mass spectrometry is by electrospray ionisation. endstream endobj 3419 0 obj <>>>/Filter/Standard/Length 128/O(&4n������i�c�\)V5x#Ӷ@so�|@JFq� �)/P -1324/R 4/StmF/StdCF/StrF/StdCF/U(�� X=3��]����'h )/V 4>> endobj 3420 0 obj <>/Metadata 79 0 R/Outlines 118 0 R/Pages 3416 0 R/StructTreeRoot 122 0 R/Type/Catalog>> endobj 3421 0 obj <>/MediaBox[0 0 595.02 841.98]/Parent 3416 0 R/Resources<>/ProcSet[/PDF/Text/ImageB/ImageC/ImageI]/XObject<>>>/Rotate 0/StructParents 0/Tabs/S/Type/Page>> endobj 3422 0 obj <>stream �Uˑ)F���:��NK>����w���O��!�~9���*rU�8�����/�I��>���Wc�I+�(��{0�i�h����8����80K4°���NC���bM�ې��3I��\�PmT��J�>��G���Y?���n�2����@7a4h�5���@J��c����T�Z"�՗$� ��ln��� 3445 0 obj <>stream a) Explain what is happening in the ionisation part of the spectrometer which looks like this in close-up: b) How are the ions produced in the ionisation chamber accelerated? 3. The most abundant one is Zr-90, followed by Zr-94 and Zr-92 which have similar abundances. Advances in mass spectrometry, including the ionization and ion-separation methods, and its applications in various branches of science and human activity are overviewed. �O�j�0��������g�O�9?6� Student guide: Time of flight mass spectrometry – example questions and answers 01.1 One of the methods of ionising samples in time of flight mass spectrometry is by electron impact. Mass spectrometry practice questions 157 ... €€€€ Ionisation is the first of the four main stages involved in obtaining the mass spectrum of a sample of gaseous titanium atoms. Data System Mass Detector Analyzer Vacuum System Source Inlet Region *More precisely mass spectrometry determines the mass of a molecule. How many peaks are on the graph? 3428 0 obj <>/Encrypt 3419 0 R/Filter/FlateDecode/ID[]/Index[3418 28]/Info 3417 0 R/Length 74/Prev 345924/Root 3420 0 R/Size 3446/Type/XRef/W[1 3 1]>>stream

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